All crucibles can be conveniently loaded or faraway from the TGA or DSC measuring mobile—possibly manually or mechanically—utilizing the sample robot. Automatic lid removal and piercing before measurment stops the uptake of dampness and sample contamination.
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The correctly flat base and very low mass make these crucibles great candidates for TGA/DSC measurements at temperatures higher than 600 °C.
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In addition, you will desire a crucible with a tough protective glaze. Harm to the glaze from tough managing can cause oxidation damage to the crucible. Extruded aluminum ingots typically have sharp edges that Slice deeply right into a crucible’s body leading to damaging cracks.
It offers aid for but won't click here substitute the necessity for metal melters and crucible suppliers to work carefully alongside one another from the crucible range approach.
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The crucible can be hermetically sealed to suppress endothermic evaporation, vaporization or sublimation when carrying out DSC measurements on risky substances. The maximum permissible overpressure the sealed click here lid withstands is 0.2 MPa.